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1 article(s) from Knittl, Monika

Microsolvation and sp²-stereoinversion of monomeric α-(2,6-di-tert-butylphenyl)vinyllithium as measured by NMR

Rudolf Knorr,
Monika Knittl and
Eva C. Rossmann

Beilstein J. Org. Chem. 2014, 10, 2521–2530, doi:10.3762/bjoc.10.263

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Scheme 1: The sterically congested model systems.

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Scheme 2: Preparation and derivatives of the α-arylvinyllithium 4, where Don = ½TMEDA and d = 2 for the purif...

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Figure 1: ¹³C and (in parentheses) ¹H NMR lithiation shifts Δδ = δ(R–Li) − δ(R–H) [ppm] of the monomers (“M”) ...

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Scheme 3: THF-catalyzed ionization of ground-state 11 (CIP) generates the solvent-separated ion pair 12 (SSIP...

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Figure 2: Arrhenius diagram of the natural logarithms of pseudo-first-order rate constants k_ψ [s⁻¹] of sp²-st...

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Published 29 Oct 2014

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Microsolvation and sp2-stereoinversion of monomeric α-(2,6-di-tert-butylphenyl)vinyllithium as measured by NMR

Microsolvation and sp²-stereoinversion of monomeric α-(2,6-di-tert-butylphenyl)vinyllithium as measured by NMR